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Process Engineering - 06 / 06

PPS Reaction Chamber

I manufactured a custom, chemical-resistant reaction vessel 3D-printed in polyphenylene sulfide (PPS) for an organic chemistry lab.

Lab
SLU Center for Additive Manufacturing
Material
PPS
For
Organic Chemistry Lab
PPS reaction chamber

Designed at the SLU Center for Additive Manufacturing, this single-piece reaction chamber integrates pump inputs, a filter outlet, and a vacuum port to automate chemical processing, replacing expensive and fragile multi-piece glass assemblies.

Why PPS

The application required polyphenylene sulfide (PPS) due to its extreme chemical resistance and high thermal stability.

Whiteboard sketch of the reaction chamber design
Whiteboarding the design
Early CAD iteration of the reaction chamber
Early CAD iteration
CAD cross-section showing the filter assembly
Filter assembly cross-section

High-Temperature PPS Printing

Because standard desktop hardware caps nozzle temperatures below PPS processing levels, I assisted the lab in modifying the thermistor resistance values on a Bambu P1S to override firmware safety limits. This allowed the hotend to maintain the higher temperatures required to extrude the material cleanly.

Finished PPS reaction chamber with fittings
Fittings and dovetail mount
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