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Process Engineering — 06 / 06

PPS Reaction Chamber

A custom reaction chamber for an organic chemistry lab — pump inputs, a filter output, and a vacuum output automating a reaction process, 3D printed in a plastic most desktop printers can't touch.

Lab
SLU Center for Additive Manufacturing
Material
PPS
For
Organic Chemistry Lab
PPS reaction chamber

This was research at the SLU Center for Additive Manufacturing: an organic chemistry lab needed a way to automate a reaction, so I designed a custom chamber around it — pump inputs to feed reagents in, a filter output, and a vacuum output, all built into one printed part instead of a rig of fittings and tubing bolted together.

Why PPS

The chamber needed to hold up to the reaction itself — chemically resistant and stable at temperatures that would soften most printable plastics. PPS (polyphenylene sulfide) handles both, which is exactly why it's a pain to print.

Whiteboard sketch of the reaction chamber design
Whiteboarding the design
Early CAD iteration of the reaction chamber
Early CAD iteration
CAD cross-section showing the filter assembly
Filter assembly, in section

Printing It

I printed the chamber on a Bambu P1S, which doesn't officially support PPS — its firmware caps the nozzle well below the temperature the material actually needs. I got around it by feeding the printer a modified thermistor reading, so it believed the nozzle was cooler than it really was and kept driving the heater past its normal ceiling. Not a supported workflow, but it printed.

Finished PPS reaction chamber with fittings
Fittings and dovetail mount
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